Annual Reports on NMR Spectroscopy, Volume 92 provides a thorough and in-depth accounting of progress in nuclear magnetic resonance (NMR) spectroscopy and its many applications. Topics presented include new chapters on The DEPT Experiment and Some of Its Useful Variants, NMR Studies of Organic Aerosols, Recent NMR Studies of Thermoelectric Materials, Nonlinear Effects in NMR, Applications of Solid-State 43 Ca Nuclear Magnetic Resonance: Superconductors, Glasses, Biomaterials, and NMR Crystallography, and Solid-State NMR Spectroscopy: The Magic Wand to View Bone at Nanoscopic Resolution.
This book has established itself as a premier means for both specialists and non-specialists who are looking to become familiar with new techniques and applications pertaining to NMR spectroscopy.
1. 1 Introduction - p. 2 2. 2 Product Operator Formalism - p. 4 3. 3 Spin Echo (SE)-Based Experiments - p. 4 4. 4 INEPT-Based Experiments - p. 15 5. 5 Basic Theory Analysis of the Standard DEPT Experiment - p. 27 6. 6 The POMMIE Experiment - p. 43 7. 7 Application of DEPT to Other Heteronuclei - p. 45 8. 8 The DEPT+ and DEPT++ Sequences - p. 49 9. 9 J-Compensated DEPT Sequences - p. 51 10. 10 The IDEPT Experiment - p. 53 11. 11 Inclusion of Quaternary Carbons: The DEPTQ Sequence - p. 56 12. 12 Equalizing the Intensities: The ACCORDEPT Experiment - p. 63 13. 13 Obtaining Quantitative 13C Spectra: The Q-DEPT and Q-DEPT+ Experiments - p. 74 14. 14 Comparison of APT, DEPT, DEPTQ, RefINEPT, and PENDANT Experiments: Conclusion and Practical Recommendations - p. 76 15. Appendix - p. 78 16. Chapter Two: NMR Studies of Organic Aerosols - p. 82 17. Chapter Three: Recent NMR Studies of Thermoelectric Materials - p. 135 18. Chapter Four: Nonlinear Effects in NMR - p. 198 19. Chapter Five: Applications of Solid-State 43Ca Nuclear Magnetic Resonance: Superconductors, Glasses, Biomaterials, and NMR Crystallography - p. 226 20. Abstract - p. 227 21. 1 Introduction and Background - p. 228 22. 2 Calcium-43 Solid-State NMR Literature Accounts - p. 263 23. 3 Calcium-43 SSNMR Prospective - p. 347 24. Acknowledgments - p. 349 25. Chapter Six: Solid-State NMR Spectroscopy: The Magic Wand to View Bone at Nanoscopic Resolution - p. 363 26. Index - p. 415
Annual Reports on NMR Spectroscopy, Volume 92 provides a thorough and in-depth accounting of progress in nuclear magnetic resonance (NMR) spectroscopy and its many applications. Topics presented include new chapters on The DEPT Experiment and Some of Its Useful Variants, NMR Studies of Organic Aerosols, Recent NMR Studies of Thermoelectric Materials, Nonlinear Effects in NMR, Applications of Solid-State 43 Ca Nuclear Magnetic Resonance: Superconductors, Glasses, Biomaterials, and NMR Crystallography, and Solid-State NMR Spectroscopy: The Magic Wand to View Bone at Nanoscopic Resolution.
This book has established itself as a premier means for both specialists and non-specialists who are looking to become familiar with new techniques and applications pertaining to NMR spectroscopy.
1. 1 Introduction - p. 2 2. 2 Product Operator Formalism - p. 4 3. 3 Spin Echo (SE)-Based Experiments - p. 4 4. 4 INEPT-Based Experiments - p. 15 5. 5 Basic Theory Analysis of the Standard DEPT Experiment - p. 27 6. 6 The POMMIE Experiment - p. 43 7. 7 Application of DEPT to Other Heteronuclei - p. 45 8. 8 The DEPT+ and DEPT++ Sequences - p. 49 9. 9 J-Compensated DEPT Sequences - p. 51 10. 10 The IDEPT Experiment - p. 53 11. 11 Inclusion of Quaternary Carbons: The DEPTQ Sequence - p. 56 12. 12 Equalizing the Intensities: The ACCORDEPT Experiment - p. 63 13. 13 Obtaining Quantitative 13C Spectra: The Q-DEPT and Q-DEPT+ Experiments - p. 74 14. 14 Comparison of APT, DEPT, DEPTQ, RefINEPT, and PENDANT Experiments: Conclusion and Practical Recommendations - p. 76 15. Appendix - p. 78 16. Chapter Two: NMR Studies of Organic Aerosols - p. 82 17. Chapter Three: Recent NMR Studies of Thermoelectric Materials - p. 135 18. Chapter Four: Nonlinear Effects in NMR - p. 198 19. Chapter Five: Applications of Solid-State 43Ca Nuclear Magnetic Resonance: Superconductors, Glasses, Biomaterials, and NMR Crystallography - p. 226 20. Abstract - p. 227 21. 1 Introduction and Background - p. 228 22. 2 Calcium-43 Solid-State NMR Literature Accounts - p. 263 23. 3 Calcium-43 SSNMR Prospective - p. 347 24. Acknowledgments - p. 349 25. Chapter Six: Solid-State NMR Spectroscopy: The Magic Wand to View Bone at Nanoscopic Resolution - p. 363 26. Index - p. 415
