Applications of High Resolution Mass Spectrometry: Food Safety and Pesticide Residue Analysis is the first book to offer complete coverage of all aspects of high resolution mass spectrometry (HRMS) used for the analysis of pesticide residue in food. Aimed at researchers and graduate students in food safety, toxicology, and analytical chemistry, the book equips readers with foundational knowledge of HRMS, including established and state-of-the-art principles and analysis strategies. Additionally, it provides a roadmap for implementation, including discussions of the latest instrumentation and software available.
Detailed coverage is given to the application of HRMS coupled to ultra high-performance liquid chromatography (UHPLC-HRMS) in the analysis of pesticide residue in fruits and vegetables and food from animal origin.
The book also discusses extraction procedures and the challenges of sample preparation, gas chromatography coupled to high resolution mass spectrometry, flow injection-HRMS, ambient ionization, and identification of pesticide transformation products in food. Responding to the fast development and application of these new procedures, this book is an essential resource in the food safety field.
1. Cover image - p. i 2. Title page - p. ii 3. Table of Contents - p. iii 4. Copyright - p. iv 5. List of Contributors - p. xi 6. Preface - p. xiii 7. Chapter 1. HRMS: Fundamentals and Basic Concepts - p. 1 8. Chapter 2. HRMS: Hardware and Software - p. 15 9. Chapter 3. Analytical Strategies Used in HRMS - p. 59 10. Chapter 4. Current Legislation on Pesticides - p. 83 11. Chapter 5. Advanced Sample Preparation Techniques for Pesticide Residues Determination by HRMS Analysis - p. 131 12. Chapter 6. Applications of Liquid Chromatography Coupled With High-Resolution Mass Spectrometry for Pesticide Residue Analysis in Fruit and Vegetable Matrices - p. 165 13. Chapter 7. Application of HRMS in Pesticide Residue Analysis in Food From Animal Origin - p. 203 14. Chapter 8. Recent Advances in HRMS Analysis of Pesticide Residues Using Atmospheric Pressure Gas Chromatography and Ion Mobility - p. 233 15. Chapter 9. Direct Analysis of Pesticides by Stand-Alone Mass Spectrometry: Flow Injection and Ambient Ionization - p. 265 16. Chapter 10. Identification of Pesticide Transformation Products in Food Applying High-Resolution Mass Spectrometry - p. 315 17. Index - p. 337
Applications of High Resolution Mass Spectrometry: Food Safety and Pesticide Residue Analysis is the first book to offer complete coverage of all aspects of high resolution mass spectrometry (HRMS) used for the analysis of pesticide residue in food. Aimed at researchers and graduate students in food safety, toxicology, and analytical chemistry, the book equips readers with foundational knowledge of HRMS, including established and state-of-the-art principles and analysis strategies. Additionally, it provides a roadmap for implementation, including discussions of the latest instrumentation and software available.
Detailed coverage is given to the application of HRMS coupled to ultra high-performance liquid chromatography (UHPLC-HRMS) in the analysis of pesticide residue in fruits and vegetables and food from animal origin.
The book also discusses extraction procedures and the challenges of sample preparation, gas chromatography coupled to high resolution mass spectrometry, flow injection-HRMS, ambient ionization, and identification of pesticide transformation products in food. Responding to the fast development and application of these new procedures, this book is an essential resource in the food safety field.
1. Cover image - p. i 2. Title page - p. ii 3. Table of Contents - p. iii 4. Copyright - p. iv 5. List of Contributors - p. xi 6. Preface - p. xiii 7. Chapter 1. HRMS: Fundamentals and Basic Concepts - p. 1 8. Chapter 2. HRMS: Hardware and Software - p. 15 9. Chapter 3. Analytical Strategies Used in HRMS - p. 59 10. Chapter 4. Current Legislation on Pesticides - p. 83 11. Chapter 5. Advanced Sample Preparation Techniques for Pesticide Residues Determination by HRMS Analysis - p. 131 12. Chapter 6. Applications of Liquid Chromatography Coupled With High-Resolution Mass Spectrometry for Pesticide Residue Analysis in Fruit and Vegetable Matrices - p. 165 13. Chapter 7. Application of HRMS in Pesticide Residue Analysis in Food From Animal Origin - p. 203 14. Chapter 8. Recent Advances in HRMS Analysis of Pesticide Residues Using Atmospheric Pressure Gas Chromatography and Ion Mobility - p. 233 15. Chapter 9. Direct Analysis of Pesticides by Stand-Alone Mass Spectrometry: Flow Injection and Ambient Ionization - p. 265 16. Chapter 10. Identification of Pesticide Transformation Products in Food Applying High-Resolution Mass Spectrometry - p. 315 17. Index - p. 337