Pharmaceutical analysis determines the purity, concentration, active compounds, shelf life, rate of absorption in the body, identity, stability, rate of release etc. of a drug. Testing a pharmaceutical product involves a variety of chemical, physical and microbiological analyses. It is reckoned that over £10 billion is spent annually in the UK alone on pharmaceutical analysis, and the analytical processes described in this book are used in industries as diverse as food, beverages, cosmetics, detergents, metals, paints, water, agrochemicals, biotechnological products and pharmaceuticals.
This is the key textbook in pharmaceutical analysis, now revised and updated for its fourth edition.
1. Cover image - p. i 2. Title Page - p. i 3. Table of Contents - p. i 4. Copyright - p. iv 5. Preface - p. v 6. Learning resources - p. xiii 7. 1 Control of the quality of analytical methods - p. 1 8. 2 Physical and chemical properties of drug molecules - p. 26 9. 3 Titrimetric and chemical analysis methods - p. 58 10. 4 Ultraviolet and visible spectroscopy - p. 88 11. 5 Infrared spectrophotometry - p. 113 12. 6 Atomic spectrophotometry - p. 136 13. 7 Molecular emission spectroscopy - p. 150 14. 8 Nuclear magnetic resonance spectroscopy - p. 163 15. 9 Mass spectrometry - p. 200 16. 10 Chromatographic theory - p. 248 17. 11 Gas chromatography - p. 261 18. 12 High-performance liquid chromatography - p. 296 19. 13 Thin-layer chromatography - p. 351 20. 14 High-performance capillary electrophoresis - p. 368 21. 15 Extraction methods in pharmaceutical analysis - p. 389 22. 16 Methods used in the quality control of biotechnologically produced drugs - p. 406 23. 17 Electrochemical biosensors - p. 435 24. Answers to Self-tests - p. e1 25. Index - p. 448
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Pharmaceutical analysis determines the purity, concentration, active compounds, shelf life, rate of absorption in the body, identity, stability, rate of release etc. of a drug. Testing a pharmaceutical product involves a variety of chemical, physical and microbiological analyses. It is reckoned that over £10 billion is spent annually in the UK alone on pharmaceutical analysis, and the analytical processes described in this book are used in industries as diverse as food, beverages, cosmetics, detergents, metals, paints, water, agrochemicals, biotechnological products and pharmaceuticals.
This is the key textbook in pharmaceutical analysis, now revised and updated for its fourth edition.
1. Cover image - p. i 2. Title Page - p. i 3. Table of Contents - p. i 4. Copyright - p. iv 5. Preface - p. v 6. Learning resources - p. xiii 7. 1 Control of the quality of analytical methods - p. 1 8. 2 Physical and chemical properties of drug molecules - p. 26 9. 3 Titrimetric and chemical analysis methods - p. 58 10. 4 Ultraviolet and visible spectroscopy - p. 88 11. 5 Infrared spectrophotometry - p. 113 12. 6 Atomic spectrophotometry - p. 136 13. 7 Molecular emission spectroscopy - p. 150 14. 8 Nuclear magnetic resonance spectroscopy - p. 163 15. 9 Mass spectrometry - p. 200 16. 10 Chromatographic theory - p. 248 17. 11 Gas chromatography - p. 261 18. 12 High-performance liquid chromatography - p. 296 19. 13 Thin-layer chromatography - p. 351 20. 14 High-performance capillary electrophoresis - p. 368 21. 15 Extraction methods in pharmaceutical analysis - p. 389 22. 16 Methods used in the quality control of biotechnologically produced drugs - p. 406 23. 17 Electrochemical biosensors - p. 435 24. Answers to Self-tests - p. e1 25. Index - p. 448
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