Purification of Laboratory Chemicals, Eighth Edition, tabulates methods taken from literature for purifying thousands of individual commercially available chemicals. To help in applying this information, the more common processes currently used for purification in chemical laboratories and new methods are discussed. For dealing with substances not separately listed, a chapter is included setting out the usual methods for purifying specific classes of compounds.
1. Introduction - p. 1 2. The Question of Purity - p. 1 3. Safety Precautions Associated with the Purification of Laboratory Chemicals - p. 4 4. Methods of Purification of Reagents and Solvents - p. 7 5. Useful Websites - p. 40 6. Chapter 2: Chemical Methods Used in Purification - p. 71 7. Chapter 3: Purification of Organic Chemicals - p. 95 8. Abstract - p. 95 9. Introduction - p. 95 10. Aliphatic Compounds - p. 95 11. Alicyclic Compounds - p. 227 12. Aromatic Compounds - p. 279 13. Heterocyclic Compounds - p. 437 14. Miscellaneous As, B, P, Si, S, Se and Te Compounds - p. 551 15. Chapter 4: Purification of Inorganic and Metal-Organic Chemicals - p. 635 16. Abstract - p. 635 17. Introduction - p. 635 18. Inorganic Compounds - p. 635 19. Highly Toxic - p. 648 20. Metal-Organic Compounds - p. 725 21. Chapter 5: Catalysts - p. 771 22. Abstract - p. 771 23. Introduction - p. 771 24. Catalysts—Part 1 - p. 771 25. Catalysts—Part 2 - p. 837 26. Chapter 6: Purification of Biochemicals - p. 877 27. Abstract - p. 877 28. Introduction - p. 877 29. AMINO ACIDS and PEPTIDES - p. 885 30. Proteins, enzymes, DNA and RNA - p. 919 31. Carbohydrates - p. 939 32. Carotenoids - p. 962 33. Steroids - p. 972 34. Chapter 7: Nanomaterials and Nanotechnology - p. 1065 35. Abstract - p. 1065 36. Introduction - p. 1065 37. Identification and Measurement of Nanomaterials - p. 1065 38. Fullerenes and Related Substances - p. 1066 39. Carbon Nanotubes (CNTs) and Related Materials - p. 1074 40. Graphene Materials - p. 1086 41. Self Assembled Monolayers (SAMs) - p. 1088 42. Diamond Nanomaterials - p. 1089 43. Solvent Resistant Nano Filters (SRNF) - p. 1089 44. Nano Metals and Metal Derivatives - p. 1090 45. Some Organic and Metal-Organic Compounds Used in Nanotechnology - p. 1101 46. Safety Issues - p. 1104 47. General Index - p. 1107 48. CAS Registry Numbers Index - p. 1128
Purification of Laboratory Chemicals, Eighth Edition, tabulates methods taken from literature for purifying thousands of individual commercially available chemicals. To help in applying this information, the more common processes currently used for purification in chemical laboratories and new methods are discussed. For dealing with substances not separately listed, a chapter is included setting out the usual methods for purifying specific classes of compounds.
1. Introduction - p. 1 2. The Question of Purity - p. 1 3. Safety Precautions Associated with the Purification of Laboratory Chemicals - p. 4 4. Methods of Purification of Reagents and Solvents - p. 7 5. Useful Websites - p. 40 6. Chapter 2: Chemical Methods Used in Purification - p. 71 7. Chapter 3: Purification of Organic Chemicals - p. 95 8. Abstract - p. 95 9. Introduction - p. 95 10. Aliphatic Compounds - p. 95 11. Alicyclic Compounds - p. 227 12. Aromatic Compounds - p. 279 13. Heterocyclic Compounds - p. 437 14. Miscellaneous As, B, P, Si, S, Se and Te Compounds - p. 551 15. Chapter 4: Purification of Inorganic and Metal-Organic Chemicals - p. 635 16. Abstract - p. 635 17. Introduction - p. 635 18. Inorganic Compounds - p. 635 19. Highly Toxic - p. 648 20. Metal-Organic Compounds - p. 725 21. Chapter 5: Catalysts - p. 771 22. Abstract - p. 771 23. Introduction - p. 771 24. Catalysts—Part 1 - p. 771 25. Catalysts—Part 2 - p. 837 26. Chapter 6: Purification of Biochemicals - p. 877 27. Abstract - p. 877 28. Introduction - p. 877 29. AMINO ACIDS and PEPTIDES - p. 885 30. Proteins, enzymes, DNA and RNA - p. 919 31. Carbohydrates - p. 939 32. Carotenoids - p. 962 33. Steroids - p. 972 34. Chapter 7: Nanomaterials and Nanotechnology - p. 1065 35. Abstract - p. 1065 36. Introduction - p. 1065 37. Identification and Measurement of Nanomaterials - p. 1065 38. Fullerenes and Related Substances - p. 1066 39. Carbon Nanotubes (CNTs) and Related Materials - p. 1074 40. Graphene Materials - p. 1086 41. Self Assembled Monolayers (SAMs) - p. 1088 42. Diamond Nanomaterials - p. 1089 43. Solvent Resistant Nano Filters (SRNF) - p. 1089 44. Nano Metals and Metal Derivatives - p. 1090 45. Some Organic and Metal-Organic Compounds Used in Nanotechnology - p. 1101 46. Safety Issues - p. 1104 47. General Index - p. 1107 48. CAS Registry Numbers Index - p. 1128
