Supercritical fluid chromatography (SFC) is a rapidly developing laboratory technique for the separation and identification of compounds in mixtures. Recent, significant improvements in instrumentation have rekindled interest in SFC and have enhanced its standing in the scientific community. Many scientists are familiar with column liquid chromatography and its potential beyond traditional liquid chromatography, yet many of its capabilities remain underappreciated. Supercritical Fluid Chromatography and Extraction explores contemporary supercritical fluid chromatography and extraction and how it should be implemented in laboratory science for analysis, isolation, and production.
New to This Edition
This new edition details recent advances and applications of supercritical fluids in sample prep, instrumental analysis, and process-scale, including SFE, making it a comprehensive resource for both techniques. Further enhancements to this edition include:
1. Title of Book - p. i 2. Cover image - p. i 3. Title page - p. ii 4. Table of Contents - p. iii 5. Copyright - p. iv 6. List of contributors - p. xiii 7. 1. Core concepts and milestones in the development of supercritical fluid chromatography - p. 1 8. 2. Theory of supercritical fluid chromatography - p. 33 9. 3. Stationary phases for achiral supercritical fluid chromatography - p. 67 10. 4. Stationary phases for the separation of stereoisomers by supercritical fluid chromatography - p. 95 11. 5. Mobile phase modifiers and additives in supercritical fluid chromatography - p. 117 12. 6. Method development in supercritical fluid chromatography - p. 149 13. 7. Instrument platforms for analytical supercritical fluid chromatography - p. 173 14. 8. Fundamentals and specific behaviors of numerous detectors in supercritical fluid chromatography - p. 197 15. 9. Mass spectrometric detection in supercritical fluid chromatography - p. 215 16. 10. Multidimensional supercritical fluid chromatography - p. 245 17. 11. Validation of supercritical fluid chromatographic methods - p. 261 18. 12. Sample preparation for biological samples for supercritical fluid chromatography - p. 295 19. 13. Supercritical fluid chromatography of amino acids, peptides, and proteins - p. 309 20. 14. Supercritical fluid chromatography of lipids - p. 331 21. 15. Supercritical fluid chromatography of stereoisomers - p. 353 22. 16. Applications of supercritical fluid chromatography in environmental analysis - p. 393 23. 17. Application of supercritical fluid chromatography in food analysis - p. 419 24. 18. Applications of supercritical fluid chromatography in forensic analysis with special focus on new psychoactive substances - p. 443 25. 19. Applications of supercritical fluid chromatography in natural product analysis - p. 467 26. 20. Applications of supercritical fluid chromatography for the analysis of petroleum products - p. 489 27. 21. Applications of supercritical fluid chromatography in the pharmaceutical industry - p. 521 28. 22. Theories for preparative supercritical fluid chromatography - p. 541 29. 23. Practical aspects of preparative supercritical fluid chromatography - p. 565 30. 24. A journey to the core concepts and fundamentals of Supercritical Fluid Extraction - p. 583 31. 25. Instrument platforms for supercritical fluid extraction - p. 625 32. 26. Comparing supercritical fluid extraction with pressurized liquid extraction - p. 657 33. 27. Supercritical fluid extraction of agricultural products - p. 679 34. 28. Supercritical fluid extraction of petrochemicals from geochemical sources - p. 719 35. 29. Supercritical fluid extraction of environmental samples - p. 741 36. Index - p. 771
Supercritical fluid chromatography (SFC) is a rapidly developing laboratory technique for the separation and identification of compounds in mixtures. Recent, significant improvements in instrumentation have rekindled interest in SFC and have enhanced its standing in the scientific community. Many scientists are familiar with column liquid chromatography and its potential beyond traditional liquid chromatography, yet many of its capabilities remain underappreciated. Supercritical Fluid Chromatography and Extraction explores contemporary supercritical fluid chromatography and extraction and how it should be implemented in laboratory science for analysis, isolation, and production.
New to This Edition
This new edition details recent advances and applications of supercritical fluids in sample prep, instrumental analysis, and process-scale, including SFE, making it a comprehensive resource for both techniques. Further enhancements to this edition include:
1. Title of Book - p. i 2. Cover image - p. i 3. Title page - p. ii 4. Table of Contents - p. iii 5. Copyright - p. iv 6. List of contributors - p. xiii 7. 1. Core concepts and milestones in the development of supercritical fluid chromatography - p. 1 8. 2. Theory of supercritical fluid chromatography - p. 33 9. 3. Stationary phases for achiral supercritical fluid chromatography - p. 67 10. 4. Stationary phases for the separation of stereoisomers by supercritical fluid chromatography - p. 95 11. 5. Mobile phase modifiers and additives in supercritical fluid chromatography - p. 117 12. 6. Method development in supercritical fluid chromatography - p. 149 13. 7. Instrument platforms for analytical supercritical fluid chromatography - p. 173 14. 8. Fundamentals and specific behaviors of numerous detectors in supercritical fluid chromatography - p. 197 15. 9. Mass spectrometric detection in supercritical fluid chromatography - p. 215 16. 10. Multidimensional supercritical fluid chromatography - p. 245 17. 11. Validation of supercritical fluid chromatographic methods - p. 261 18. 12. Sample preparation for biological samples for supercritical fluid chromatography - p. 295 19. 13. Supercritical fluid chromatography of amino acids, peptides, and proteins - p. 309 20. 14. Supercritical fluid chromatography of lipids - p. 331 21. 15. Supercritical fluid chromatography of stereoisomers - p. 353 22. 16. Applications of supercritical fluid chromatography in environmental analysis - p. 393 23. 17. Application of supercritical fluid chromatography in food analysis - p. 419 24. 18. Applications of supercritical fluid chromatography in forensic analysis with special focus on new psychoactive substances - p. 443 25. 19. Applications of supercritical fluid chromatography in natural product analysis - p. 467 26. 20. Applications of supercritical fluid chromatography for the analysis of petroleum products - p. 489 27. 21. Applications of supercritical fluid chromatography in the pharmaceutical industry - p. 521 28. 22. Theories for preparative supercritical fluid chromatography - p. 541 29. 23. Practical aspects of preparative supercritical fluid chromatography - p. 565 30. 24. A journey to the core concepts and fundamentals of Supercritical Fluid Extraction - p. 583 31. 25. Instrument platforms for supercritical fluid extraction - p. 625 32. 26. Comparing supercritical fluid extraction with pressurized liquid extraction - p. 657 33. 27. Supercritical fluid extraction of agricultural products - p. 679 34. 28. Supercritical fluid extraction of petrochemicals from geochemical sources - p. 719 35. 29. Supercritical fluid extraction of environmental samples - p. 741 36. Index - p. 771
