Practical Aspects of Electroorganic Synthesis presents educational insights into the practical aspects of electrosynthesis methods, providing a variety of examples and techniques. The book covers concepts referred to as "green chemistry" and "sustainable technology." Sections cover direct electrolysis, anodic oxidation, cathodic reduction, mechanistic studies (cyclic voltammetry), and how to set-up electrochemical experiments. Indirect electrolysis is also covered, including an exploration of catalysts and additives to take on modern electrochemical methods. Finally, the book explores the burgeoning new field of paired electrolysis, in which the ultimate green-synthesis applications are possible, with no wasted electrons and very few by-products.
This book offers researchers a modern and authoritative resource that brings complete and up-to-date practical concepts of electrosynthesis methods and guides the audience on how to carry out a large number of experimental techniques.
1. Chapter 1 Introduction - p. 1 2. 1.1: Introduction to electrosynthesis - p. 1 3. 1.2: Electrosynthesis methods: direct and indirect methods - p. 3 4. 1.3: Electrosynthesis methods: controlled potential and galvanostatic methods - p. 4 5. 1.4: Electrochemical cells - p. 5 6. 1.5: Electrodes - p. 7 7. 1.6: Solvents - p. 9 8. 1.7: Supporting electrolyte - p. 14 9. 1.8: Green aspects of electroorganic synthesis - p. 15 10. 1.9: Paired electrosynthesis - p. 16 11. 1.10: Cation-pool electrosynthesis - p. 25 12. 1.11: Introduction to electrochemical methods - p. 26 13. Chapter 2 Direct electrosynthesis reactions - p. 81 14. Chapter 3 In-direct electrosynthesis reactions - p. 137 15. Chapter 4 Paired electroorganic synthesis - p. 185 16. Chapter 5 Diels–Alder reaction in electroorganic synthesis - p. 221 17. Chapter 6 Michael addition reaction in electroorganic synthesis - p. 248 18. Chapter 7 Electrosynthesis of metal-organic frameworks - p. 286 19. Index - p. 327
Practical Aspects of Electroorganic Synthesis presents educational insights into the practical aspects of electrosynthesis methods, providing a variety of examples and techniques. The book covers concepts referred to as "green chemistry" and "sustainable technology." Sections cover direct electrolysis, anodic oxidation, cathodic reduction, mechanistic studies (cyclic voltammetry), and how to set-up electrochemical experiments. Indirect electrolysis is also covered, including an exploration of catalysts and additives to take on modern electrochemical methods. Finally, the book explores the burgeoning new field of paired electrolysis, in which the ultimate green-synthesis applications are possible, with no wasted electrons and very few by-products.
This book offers researchers a modern and authoritative resource that brings complete and up-to-date practical concepts of electrosynthesis methods and guides the audience on how to carry out a large number of experimental techniques.
1. Chapter 1 Introduction - p. 1 2. 1.1: Introduction to electrosynthesis - p. 1 3. 1.2: Electrosynthesis methods: direct and indirect methods - p. 3 4. 1.3: Electrosynthesis methods: controlled potential and galvanostatic methods - p. 4 5. 1.4: Electrochemical cells - p. 5 6. 1.5: Electrodes - p. 7 7. 1.6: Solvents - p. 9 8. 1.7: Supporting electrolyte - p. 14 9. 1.8: Green aspects of electroorganic synthesis - p. 15 10. 1.9: Paired electrosynthesis - p. 16 11. 1.10: Cation-pool electrosynthesis - p. 25 12. 1.11: Introduction to electrochemical methods - p. 26 13. Chapter 2 Direct electrosynthesis reactions - p. 81 14. Chapter 3 In-direct electrosynthesis reactions - p. 137 15. Chapter 4 Paired electroorganic synthesis - p. 185 16. Chapter 5 Diels–Alder reaction in electroorganic synthesis - p. 221 17. Chapter 6 Michael addition reaction in electroorganic synthesis - p. 248 18. Chapter 7 Electrosynthesis of metal-organic frameworks - p. 286 19. Index - p. 327
