Sample Handling and Trace Analysis of Pollutants: Innovations to Determine Organic Contaminants, Second Edition reviews the latest technologies and challenges in trace analysis of environmental pollutants, from selecting the right approach to tips for performing analytic procedures and measuring and reporting results. Written by internationally renowned experts in environmental analysis from 5 continents and edited by leaders in the field, this completely updated and revised volume presents the latest techniques developed over the past 10 years, such as high-resolution mass spectrometry, biosensors and imaging techniques. Important tools for problem-solving in the determination of environmental pollutants are also discussed.Chapters cover emerging pollutants in the environment, such as nanomaterials, microplastics, metabolites and/or transformation products and antimicrobial resistances. Specific sections describe field sampling techniques and sample preparation in environmental matrices: air, water, soil, sediment and biota, focus on passive samplers, cover the determination of these environmental contaminants based on analytical techniques, such as the use of gas chromatography and liquid chromatography coupled to mass spectrometry, immunoassays, and biosensors as well as advanced analytical methods such as imaging techniques.
1. Title of Book - p. i 2. Cover image - p. i 3. Title page - p. ii 4. Table of Contents - p. iii 5. Copyright - p. iii 6. Contributors - p. xiii 7. Section I: Field sampling techniques, sample preparation and extraction - p. xviii 8. Chapter 1. Analytical methods for determining organic compounds in air - p. 3 9. Chapter 2. Extraction of organic contaminants from grab and composite water samples - p. 35 10. Chapter 3. Extraction, cleanup and recovery of trace organic pollutants in biota - p. 65 11. Chapter 4. Handling of food samples - p. 135 12. Section II: Trace analysis of organic pollutants - p. 169 13. Chapter 5. Liquid chromatography-mass spectrometry - p. 181 14. Chapter 6. HRMS-based suspect and non-target screening for contaminants of emerging concern: Current analytical strategies, compounds identification workflows, general research trends, and future perspectives - p. 213 15. Chapter 7. Imaging techniques: The increasing role of mass spectrometry imaging in environmental science - p. 259 16. Chapter 8. Immunoassays of organic contaminants - p. 299 17. Chapter 9. Fundamentals and applications of biosensors for environmental analysis - p. 325 18. Chapter 10. The role of nanomaterials and nanoparticles as analytical tools - p. 345 19. Section III: Quality assurance, reference materials, chemometrics and data dissemination - p. 369 20. Chapter 11. Certified reference materials for environmental monitoring of organic contaminants - p. 379 21. Chapter 12. Standard reference materials for the determination of trace organic constituents in environmental samples - p. 417 22. Chapter 13. Guidelines to establish the quality assurance, analytical parameters, and inter-laboratory studies - p. 435 23. Chapter 14. Data dissemination and repositories - p. 457 24. Section IV: New application areas - p. 470 25. Chapter 15. Wastewater-derived contaminants of emerging concern in the water-soil-plant continuum - p. 477 26. Chapter 16. Endocrine disrupting chemicals in freshwater envrionments - p. 507 27. Chapter 17. Current issues in micro- and nanoplastic research - p. 563 28. Chapter 18. Determination of microplastics in soil and sludge - p. 585 29. Chapter 19. Determination of nanomaterials in the environment - p. 621 30. Chapter 20. Detection of antibiotic resistance genes in wastewater and sludge - p. 651 31. Chapter 21. Identification of metabolites and transformation products of environmental contaminants - p. 663 32. Chapter 22. The anthropic fingerprinting of chemicals in wastewater: Wastewater based-epidemiology - p. 691 33. Chapter 23. Advanced sensors enabled rapid and on-site wastewater surveillance for SARS-CoV-2 and beyond - p. 719 34. Chapter 24. Green analytical chemistry - p. 739 35. Index - p. 773
Sample Handling and Trace Analysis of Pollutants: Innovations to Determine Organic Contaminants, Second Edition reviews the latest technologies and challenges in trace analysis of environmental pollutants, from selecting the right approach to tips for performing analytic procedures and measuring and reporting results. Written by internationally renowned experts in environmental analysis from 5 continents and edited by leaders in the field, this completely updated and revised volume presents the latest techniques developed over the past 10 years, such as high-resolution mass spectrometry, biosensors and imaging techniques. Important tools for problem-solving in the determination of environmental pollutants are also discussed.Chapters cover emerging pollutants in the environment, such as nanomaterials, microplastics, metabolites and/or transformation products and antimicrobial resistances. Specific sections describe field sampling techniques and sample preparation in environmental matrices: air, water, soil, sediment and biota, focus on passive samplers, cover the determination of these environmental contaminants based on analytical techniques, such as the use of gas chromatography and liquid chromatography coupled to mass spectrometry, immunoassays, and biosensors as well as advanced analytical methods such as imaging techniques.
1. Title of Book - p. i 2. Cover image - p. i 3. Title page - p. ii 4. Table of Contents - p. iii 5. Copyright - p. iii 6. Contributors - p. xiii 7. Section I: Field sampling techniques, sample preparation and extraction - p. xviii 8. Chapter 1. Analytical methods for determining organic compounds in air - p. 3 9. Chapter 2. Extraction of organic contaminants from grab and composite water samples - p. 35 10. Chapter 3. Extraction, cleanup and recovery of trace organic pollutants in biota - p. 65 11. Chapter 4. Handling of food samples - p. 135 12. Section II: Trace analysis of organic pollutants - p. 169 13. Chapter 5. Liquid chromatography-mass spectrometry - p. 181 14. Chapter 6. HRMS-based suspect and non-target screening for contaminants of emerging concern: Current analytical strategies, compounds identification workflows, general research trends, and future perspectives - p. 213 15. Chapter 7. Imaging techniques: The increasing role of mass spectrometry imaging in environmental science - p. 259 16. Chapter 8. Immunoassays of organic contaminants - p. 299 17. Chapter 9. Fundamentals and applications of biosensors for environmental analysis - p. 325 18. Chapter 10. The role of nanomaterials and nanoparticles as analytical tools - p. 345 19. Section III: Quality assurance, reference materials, chemometrics and data dissemination - p. 369 20. Chapter 11. Certified reference materials for environmental monitoring of organic contaminants - p. 379 21. Chapter 12. Standard reference materials for the determination of trace organic constituents in environmental samples - p. 417 22. Chapter 13. Guidelines to establish the quality assurance, analytical parameters, and inter-laboratory studies - p. 435 23. Chapter 14. Data dissemination and repositories - p. 457 24. Section IV: New application areas - p. 470 25. Chapter 15. Wastewater-derived contaminants of emerging concern in the water-soil-plant continuum - p. 477 26. Chapter 16. Endocrine disrupting chemicals in freshwater envrionments - p. 507 27. Chapter 17. Current issues in micro- and nanoplastic research - p. 563 28. Chapter 18. Determination of microplastics in soil and sludge - p. 585 29. Chapter 19. Determination of nanomaterials in the environment - p. 621 30. Chapter 20. Detection of antibiotic resistance genes in wastewater and sludge - p. 651 31. Chapter 21. Identification of metabolites and transformation products of environmental contaminants - p. 663 32. Chapter 22. The anthropic fingerprinting of chemicals in wastewater: Wastewater based-epidemiology - p. 691 33. Chapter 23. Advanced sensors enabled rapid and on-site wastewater surveillance for SARS-CoV-2 and beyond - p. 719 34. Chapter 24. Green analytical chemistry - p. 739 35. Index - p. 773
