Vapor Generation Techniques for Trace Element Analysis: Fundamental Aspects provides an overview and discussion of the fundamental aspects governing derivatization reactions of trace-level elements for analytical purposes. Vapor generation techniques coupled with atomic or mass spectrometry have been employed for over 50 years, but their popularity has dramatically increased in recent years, especially as alternative vapor generation approaches have been developed. This book bridges the knowledge gap of the derivatization mechanisms that yield volatile compounds and provides an update on recent developments in vapor generation techniques used for the determination and speciation of trace elements by atomic optical and mass spectrometry.
It will serve as a comprehensive, single-source overview of recent developments, providing readers with an understanding of the correct implementation—and limitations—of applying vapor generation techniques to everyday analytical problems facing the trace element analyst.
1. Chapter 1 : Introduction to vapor generation techniques - p. Page xii 2. Chapter 2 : Chemical vapor generation by aqueous boranes - p. Page 12 3. Chapter 3 : Chemical vapor generation of transition and noble metals - p. Page 74 4. Chapter 4 : Chemical vapor generation by aqueous phase alkylation - p. Page 122 5. Chapter 5 : Other chemical vapor generation techniques - p. Page 145 6. Chapter 6 : Chemical vapor generation in nonaqueous media - p. Page 180 7. Chapter 7 : Photo-sono-thermo-chemical vapor generation techniques - p. Page 207 8. Chapter 8 : Catalysts in photochemical vapor generation - p. Page 252 9. Chapter 9 : Plasma-mediated vapor generation techniques - p. Page 276 10. Chapter 10 : Electrochemical vapor generation - p. Page 311 11. Chapter 11 : Nonplasma devices for atomization and detection of volatile metal species by atomic absorption and fluorescence - p. Page 339 12. Chapter 12 : Dielectric barrier discharge devices - p. Page 392 13. Abbreviations and symbols - p. Page 437 14. Index - p. Page 446
Vapor Generation Techniques for Trace Element Analysis: Fundamental Aspects provides an overview and discussion of the fundamental aspects governing derivatization reactions of trace-level elements for analytical purposes. Vapor generation techniques coupled with atomic or mass spectrometry have been employed for over 50 years, but their popularity has dramatically increased in recent years, especially as alternative vapor generation approaches have been developed. This book bridges the knowledge gap of the derivatization mechanisms that yield volatile compounds and provides an update on recent developments in vapor generation techniques used for the determination and speciation of trace elements by atomic optical and mass spectrometry.
It will serve as a comprehensive, single-source overview of recent developments, providing readers with an understanding of the correct implementation—and limitations—of applying vapor generation techniques to everyday analytical problems facing the trace element analyst.
1. Chapter 1 : Introduction to vapor generation techniques - p. Page xii 2. Chapter 2 : Chemical vapor generation by aqueous boranes - p. Page 12 3. Chapter 3 : Chemical vapor generation of transition and noble metals - p. Page 74 4. Chapter 4 : Chemical vapor generation by aqueous phase alkylation - p. Page 122 5. Chapter 5 : Other chemical vapor generation techniques - p. Page 145 6. Chapter 6 : Chemical vapor generation in nonaqueous media - p. Page 180 7. Chapter 7 : Photo-sono-thermo-chemical vapor generation techniques - p. Page 207 8. Chapter 8 : Catalysts in photochemical vapor generation - p. Page 252 9. Chapter 9 : Plasma-mediated vapor generation techniques - p. Page 276 10. Chapter 10 : Electrochemical vapor generation - p. Page 311 11. Chapter 11 : Nonplasma devices for atomization and detection of volatile metal species by atomic absorption and fluorescence - p. Page 339 12. Chapter 12 : Dielectric barrier discharge devices - p. Page 392 13. Abbreviations and symbols - p. Page 437 14. Index - p. Page 446